Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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Because it can be run quickly for screening, we often run this test first.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. View more articles about Aerospace Oil and Gas Transportation. This method is preferable for chromium depletions and corrosion in intermetallic phases.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: What is your typical turnaround time?
The test uses a visual inspection of the surface of the bent specimen to determine pass or fail. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which a622 to use, what to do if a test fails, and other corrosion consulting as needed.
These tests do not practics a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Atm samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
Some specific hazards pracgice are given in The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. ASTM does not give any warranty practlce or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
Work Item s – proposed revisions of this standard.
Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. practie
Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. In SEM analysis, intergranular corrosion is clear by x dark lines where the grain boundaries are eaten away.
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. If you are not sure, please contact us for assistance. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.